Solid-state NMR Group

Publications

The links will take you to the publisher's website where you can view the text of the paper, if you have the right credentials. Otherwise, recent papers are deposited at Nottingham ePrints where they are available open access, subject to the publisher's conditions.


  • Natural fluorapatite dissolution kinetics and Mn2+ and Cr3+ metal removal from sulfate fluids at 35°C, V. Vandeginste, C. Cowan, R. L. Gomes, T. Hassan, J. Titman, J. Hazard. Mater., 389, 122150 (2020).
  • M. T. Islam, N. Sharmin, G. A. Rance, J. J. Titman, A. J. Parsons, K. M. Z. Hossain, I. Ahmed, J. Biomed. Mater. Res. B, 108, 674-686 (2020).
  • Ion exchange and binding in selenium remediation materials using DNP-enhanced solid-state NMR spectroscopy, M. Mais, J. Torroba, N. S. Barrow, S. Paul and J. J. Titman, Solid State Nucl. Magn. Reson., 98, 19-23 (2019).
  • Mammalian-Cell-Driven Polymerisation of Pyrrole, H. G. Sherman, J. M. Hicks, A. Jain, J. J. Titman, C. Alexander, S. Stolnik and F. J. Rawson, ChemBioChem., 20, 1008–1013 (2019).
  • Enhancement of Proton Conductivity in Nonporous Metal-Organic Frameworks: The Role of Framework Proton Density and Humidity, S. Pili, P. Rought, D. I. Kolokolov, L. F. Lin, I. da Silva, Y. Chen, C. Marsh, I. P. Silverwood, V. G. Sakai, M. Li, J. J. Titman, L. Knight, L.L. Daemen, A. J. Ramirez-Cuesta, C. C. Tang, A. G. Stepanov, S. Yang and M. Schroder, Chem. Mater., 30, 7593-7602 (2018).
  • Structure of Ancient Glass by 29Si Magic Angle Spinning NMR Spectroscopy, H. Bradford, A. Ryder, J. Henderson and J. J. Titman, Chem. Eur. J., 24, 7474–7479 (2018).
  • Dynamic Nuclear Polarization Enhanced Solid-state NMR Studies of Surface Modification of γ-Alumina, M. Mais, S. Paul, N. S. Barrow, and J. J. Titman, Johnson Matthey Technol. Rev., 62, 271–278 (2018).
  • Gallium Incorporation into Phosphate Based Glasses: Bulk and Thin Film Properties, B. W. Stuart, C. A. Grant , G. E. Stan, A. C. Popa, J. J. Titman, and D. M. Grant, J. Mech. Behav. Biomed. Mater., 82, 371-382 (2018).
  • New insights into microwave pyrolysis of biomass: Preparation of carbon-based products from pecan nutshells and their application in wastewater treatment, G. D. Jimenez, T. Monti, J. J. Titman, V. Hernandez-Montoya, S. W. Kingman and E. R. Binner, J. Anal. Appl. Pyrol., 124, 113–121 (2017).
  • 1H CSA parameters by ultrafast MAS NMR: Measurement and applications to structure refinement, H. K. Miah, R. Cresswell, D. Iuga and J. J. Titman, Solid-state Nucl. Magn. Reson., 87, 67-72 (2017).
  • Insights into structural characterisation and thermal properties of compositionally equivalent vapour-condensed and melt-quenched glasses, B. W. Stuart, J. J. Titman, M. Gimeno-Fabra, I. Ahmed, D. M. Grant, Mater. Design, 111, 174-184 (2017).
  • Organic matter chemistry controls greenhouse gas emissions from permafrost peatlands, S. Sjogersten, S. Caul, T. J. Daniell, A. P. S. Jurd, O. S. O'Sullivan, C. S. Stapleton and J. J. Titman, Soil Biol. Biochem., 98, 42-53 (2016).
  • How does dense phase CO2 influence the phase behaviour of block copolymers synthesised by dispersion polymerisation?, J. Jennings, S. P. Bassett, D. Hermida-Merino, G. Portale, W. Bras, L. Knight, J. J. Titman, T. Higuchi, H. Jinnai, and S. M. Howdle, Polym. Chem., 7, 905-916 (2016).
  • Measuring 19F shift anisotropies and 1H–19F dipolar interactions with ultrafast MAS NMR , F. Martini, H. K. Miah, D. Iuga, M. Geppi, and J. J. Titman, J. Magn. Reson., 259, 102-107 (2015).
  • Correlating structure with non-linear optical properties in xAs40Se60•(1-x)As40S60 glasses , E. R. Barney, N. S. Abdel-Moneim, J. J. Towey, J. Titman, J. E. McCarthy, H. T. Bookey, A. Kar, D. Furniss, and A. B. Seddon, Phys. Chem. Chem. Phys., 17, 6314-6327 (2015).
  • Porous Macromolecular Dihydropyridyl Frameworks Exhibiting Catalytic and Halochromic Activity , B. Xiao, T. L. Easun, A. Dhakshinamoorthy, I. Cebula, P. H. Beton, J. J. Titman, H. Garcia, K. M. Thomas and M. Schröder, J. Mater. Chem. A, 2, 19889-19896 (2014).
  • The Role of Copper(II) in the Aggregation of Human Amylin , A. Sinopoli, A. Magrì, D. Milardi, M. Pappalardo, P. Pucci, A. Flagiello, J. J. Titman, V. G. Nicoletti, G. Caruso, G. Pappalardo and G. Grasso, Metallomics, 6, 1841-1852 (2014).
  • Chemical Shift Anisotropy Measurements via Two-dimensional Experiments: Advances, J. J. Titman, eMagRes 2, 365–376 (2013).
  • Measuring Proton Shift Tensors with Ultrafast MAS NMR, H. K. Miah, D. A. Bennett, D. Iuga and J. J. Titman, J. Magn. Reson., 235, 1-5 (2013).
  • Insight into Lithium Transport in Lithium Nitridometallate Battery Materials from Muon Spin Relaxation, A. S. Powell, Z. Stoeva, J. S. Lord, R. I. Smith, D. H. Gregory and J. J Titman Phys. Chem. Chem. Phys., 15, 816-823 (2013).
  • Pore with Gate: Enhancement of the Isosteric Heat of Adsorption of Dihydrogen via Postsynthetic Cation Exchange in Metal-Organic Frameworks, S. Yang, G. S. B. Martin, J. J Titman, A. J. Blake, D. R. Allan, N. R. Champness and M. Schroeder, Inorg. Chem., 50, 9374-9384 (2011).
  • Structure, Stoichiometry and Transport Properties of Lithium Copper Nitride Battery Materials: Combined NMR and Powder Neutron Diffraction Studies, A. S. Powell, Z. Stoeva, R. I. Smith, D. H. Gregory and J. J. Titman, J. Chem. Phys. C, 13, 10641–10647. (2011).
  • Distinguishing Hydrogen Bonding Networks in α-D-galactose Using NMR Experiments and First Principles Calculations, M. Kibalchenko, D. Lee, L. Shao , M. C. Payne, J. J. Titman and J. R. Yates, Chem. Phys. Lett., 498, 270-276 (2010).
  • Solid-state Nuclear Magnetic Resonance Studies of Vinyl Polymer / Silica Colloidal Nanocomposite Particles, D. Lee, J. A. Balmer, A. Schmid, J. Tonnar, S. P. Armes and J. J. Titman, Langmuir, 26, 15592-15598 (2010).
  • Experimental Characterization of Nuclear Spin Interaction Tensors, J. J. Titman in Handbook of NMR Crystallography, eds. R. K. Harris, R. Wasylishen and M. Duer, John Wiley, Chichester (2009).
  • Measurement of Torsion Angles By Solid-state NMR: Slow-MAS Dipolar Recoupling Using COAST-C721, A. P. S. Jurd and J. J. Titman, Phys. Chem. Chem. Phys., 11, 6999-7007 (2009).
  • Chain Folding and Diffusion in Monodisperse Long n-Alkanes by Solid-state NMR, G. Grasso and J. J. Titman, Macromolecules, 42, 4178 (2009).
  • Measurements of Nuclear Spin Interaction Tensors from Wideline Spectra and by Spinning Sideband Analysis, J. J. Titman in Encyclopedia of Magnetic Resonance, eds R. K. Harris and R. Wasylishen, John Wiley, Chichester (2009).
  • Sensitive Absorptive Refocused Scalar Correlation NMR Spectroscopy in Solids, D. Lee, J. Struppe, D. W. Elliott, L. J. Mueller and J. J. Titman, Phys. Chem. Chem. Phys., 11, 3547-3553 (2009).
  • Switching on Fast Lithium Ion Conductivity in Garnets: The Structure and Transport Properties of Li3+xNd3Te2-xSbxO12, M. P. O’Callaghan, A. S. Powell, J. J. Titman, G. Z. Chen and E. J. Cussen, Chem. Mater., 20, 2360-2369 (2008).
  • Towards New Negative Electrode Materials for Li-Ion Batteries: Electrochemical Properties of LiNiN, J. Cabana, Z. Stoeva, J. J. Titman, D. H. Gregory, and M. R. Palacín, Chem. Mater., 20, 1876-1878 (2008).
  • Carbon-13 Chemical Shift Tensors Of Disaccharides: Measurement, Computation And Assignment, L. Shao, J. R. Yates, and J. J. Titman, J. Chem. Phys. A, 111, 13126-13132 (2007).
  • CAESURA Studies of Helical Jump Motions in Semi-crystalline Polymers, L. Shao and J. J. Titman, Macromol. Chem. Phys., 208, 2055-2065 (2007).
  • Chemical Shift Anisotropy Amplification, L. Shao and J. J. Titman, Prog. NMR Spectrosc., 51, 103-137, (2007).
  • Crystal Chemistry and Electronic Structure of the Metallic Lithium Ion Conductor, LiNiN, Z. Stoeva, B. Jäger, R. Gomez, S. Messaoudi, M. Ben Yahia, X. Roquefelte, G. B. Hix, W. Wolf, J. J. Titman, R. Gautier, P. Herzig and D. H. Gregory, J. Am. Chem. Soc., 129, 1912-1920 (2007).
  • CAESURA: Measurement of Slow Molecular Dynamics by Solid-state NMR Chemical Shift Anisotropy Modulation Amplification, L. Shao and J. J. Titman, J. Chem. Phys., 125, 064507 (2006).
  • Chemical Shift Anisotropy Amplification with High Amplification Factor and Improved Sensitivity, L. Shao, C. Crockford and J. J. Titman, J. Magn. Reson., 178, 155-161 (2006).
  • Theoretical Study of the Carbon-13 NMR Spectroscopy of Single-Walled Carbon Nanotubes, N. A. Besley, J. J. Titman and N. D. Wright, J. Am. Chem. Soc., 127, 17498-17953 (2005).
  • Through-space Contributions to Two-dimensional INADEQUATE NMR Spectra of Magic-angle-spinning Solids, F. Fayon, D. Massiot, M. H. Levitt, J. J. Titman, D. H. Gregory, L. Duma, L. Emsley, S. P. Brown, J. Chem. Phys., 122, 194313 (2005).
  • Investigations into the Utility of High-Surface Area Silica Pellets as Potential Solid-Phase Synthesis Supports, R. S. Timofte, J. J. Titman, L. Shao and Simon Woodward, Tetrahedron, 61, 51 (2005).
  • Formation of Molecularly Ordered Layered Mesoporous Silica via Phase Transformation of Silicate-Surfactant Composites, Y. Xia, R. Mokaya and J. J. Titman, J. Phys. Chem. B, 108, 11361-11367 (2004).
  • Evolution of Structure, Transport Properties and Magnetism in Ternary Lithium Nitridometallates, Z. Stoeva, R. Gomez, D. H. Gregory, G. Hix and J. J. Titman, Dalton Trans., 3093 (2004).
  • Fast Lithium Ion Diffusion in the Ternary Layered Nitridometallate LiNiN, Z. Stoeva, R. Gomez, A. G. Gordon, M. Allan, D. H. Gregory, G. Hix and J. J. Titman, J. Am. Chem. Soc., 126, 4066-4067 (2004).
  • Chemical Shift Anisotropy Amplification, L. Shao, C. Crockford, H. Geen, G. Grasso and J. J. Titman, J. Magn. Reson., 167, 75-86 (2004).
  • Characterization of Vinyl Polymer/Silica Colloidal Nanocomposites Using Solid State NMR Spectroscopy: Probing the Interaction between the Inorganic and Organic Phases on the Molecular Level, G. K. Agarwal, J. J. Titman, M. J. Percy and S. P. Armes, J. Phys. Chem. B, 107, 12497-12502 (2003).
  • Measurement of Orientational Order Using Chemical Shift Anisotropy Amplification, C. Crockford, H. Geen and J. J. Titman, Solid-state Nucl. Magn. Reson., 22, 298-310 (2002).
  • Electronic Structure of the Polymer Phase of CsC60: Refocused INADEQUATE Experiments, G. Grasso, T. M. de Swiet and J. J. Titman, J. Phys. Chem. B, 106, 8676-8680, (2002).
  • Two-dimensional MAS Experiments which Correlate Fast and Slow Spinning Sideband Patterns, C. Crockford, H. Geen and J. J. Titman, Chem. Phys. Lett., 344, 367-373 (2001).
  • Improved Scalar Shift Correlation NMR Spectroscopy in Solids, A. S. D. Heindrichs, H. Geen and J. J. Titman, Chem. Phys. Lett., 335, 89-96 (2001).
  • Investigation Of The Feasibility Of Amplitude-Modulated Dipolar Decoupling In Magic Angle Spinning Solid-state Nuclear Magnetic Resonance, M. Ernst, H. Geen, A. S. D. Heindrichs, Beat H. Meier and J. J. Titman, J. Phys. B: At. Mol. Opt. Phys., 33, 1-15 (2000).
  • Double-quantum Filtered Dipolar Shift Correlation NMR Spectroscopy in Rotating Solids, A. S. D. Heindrichs, H. Geen and J. J. Titman, J. Magn. Reson., 147, 68-77 (2000).
  • Electron Spin Density Distribution In The Polymer Phase of CsC60: Assignment of the NMR Spectrum, T. M. De Swiet, J. L. Yarger, T. Wagberg, J. Hone, B. Gross, M. Tomaselli, J. J. Titman, A. Zettl and M. Mehring, Phys. Rev. Lett., 84, 717-720 (2000).
  • Precipitation Of Solvent-free C60(CO2)0.95 From Conventional Solvents: A New Antisolvent Approach To Controlled Crystal Growth Using Supercritical Fluids, C. N. Field, P. A. Hamley, J. Webster, D. H. Gregory, J. J. Titman and M. Poliakoff, J. Am. Chem. Soc., 122, 2480-2488 (2000).
  • Protonic Conduction In Imidazole – A Solid-state NMR Study, B. S. Hickman, M. Mascal, J. J. Titman and I. G. Wood, J. Am. Chem. Soc., 121, 11486-11490 (1999).
  • Isotropic Mixing, Sign Discrimination And Sensitivity In Solid-state Wideline Heteronuclear Correlation Experiments, S. L. Oliver and J. J. Titman, J. Magn. Reson., 140, 235-241 (1999).
  • Spin Counting With Fast MAS, H. Geen, A. S. D. Heindrichs, B. S. Hickman, R. Graf, I. Schnell, H. W. Spiess and J. J. Titman, J. Magn. Reson., 138, 167-172 (1999).
  • Elucidation of Dipolar Coupling Networks Under Magic Angle Spinning, H. Geen, J. Gottwald, R. Graf, I. Schnell, H. W. Spiess and J. J. Titman, J. Magn. Reson., 125, 224-227 (1997).
  • Mapping of Motional Heterogeneity In Inorganic-Organic Nanocomposite Gels, M. E. Brik, J. J. Titman, J. P. Bayle and P. Judeinstein, J. Polym. Sci. Polym. Phys., 34, 2533-2542 (1996).
  • Spinning Sidebands in Fast MAS Multiple-quantum Spectra of Protons in Solids, H. Geen, J. J. Titman, J. Gottwald and H. W. Spiess, J. Magn. Reson. A, 114, 264-267, (1995).
  • Solid-state Proton Multiple-quantum NMR Spectroscopy With Fast Magic Angle Spinning, H. Geen, J. J. Titman, J. Gottwald, and H. W. Spiess, Chem. Phys. Lett., 227, 79-86 (1994).
  • Molecular Order In A Homologous Series Of Liquid-Crystalline Side Group Polymers By Multi-dimensional Carbon-13 And Silicon-29 NMR Spectroscopy, J. J. Titman, D. L. Tzou, S. Féaux de Lacroix, C. Boeffel and H. W. Spiess, Acta Polymer., 45, 204-209 (1994).
  • Spatially-resolved Two-dimensional Solid-state NMR Spectroscopy, U. Scheler, J. J. Titman, B. Blümich and H. W. Spiess, J. Magn. Reson. A, 107, 251-254 (1994).
  • Investigations of Ion-Conducting Ormlytes: Structure-Property Relationships, P. Judeinstein, J. Titman, M. Stamm, and H. Schmidt, Chem. Mater., 6, 127-134 (1994).
  • Measurement Of The Orientation Distribution In An Industrial Sample Of Poly(p-phenyleneterephthalamide) By Two- and Three-dimensional NMR Techniques, M. Wilhelm, S. Féaux de Lacroix, J. J. Titman, K. Schmidt-Rohr, and H. W. Spiess, Acta Polymer., 44, 279-284 (1993).
  • Improvement Of z-Filters And Purging Pulses By The Use Of Zero-quantum Dephasing Sequences In Inhomogeneous B1 And B0 Fields, A. L. Davis, G. Estcourt, E. D. Laue, J. Keeler, and J. J. Titman, J. Magn. Reson. A, 105, 167-183 (1993).
  • Heteronuclear Magnetization Transfer In Rapidly Rotating Solids, H. Geen, J. J. Titman and H. W. Spiess, Chem. Phys. Lett., 213, 145-152 (1993).
  • Detection Of Structural Heterogeneity In Amorphous CH Films By NMR, C. Jäger, J. J. Titman, and R. J. Newport, Thin Solid Films, 227, 3-6 (1993).
  • The Incorporation Of C60 In Molecular Sieves, A. Gürgel, K. Müllen, H. Reichert, W. Schmidt, G. Schön, F. Schüth, J. Spickermann, J. Titman and K. Unger, Angew. Chem. Intl. Ed. Eng., 32, 556-557 (1993).
  • Structure And Order In Partially Oriented Solids By Three-Dimensional Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy, J. J. Titman, S. Féaux de Lacroix and H. W. Spiess, J. Chem. Phys., 98, 3816-3826 (1993).
  • Rotor Synchronized MAS Two-dimensional Exchange NMR. Principles and Applications, Z. Luz, H. W. Spiess and J. J. Titman, Isr. J. Chem., 32, 145-160 (1992).
  • Solid-state Reactions Studied By Carbon-13 Rotor-Synchronized Magic Angle Spinning Two-dimensional Exchange NMR 1. Self-Diffusion And The Tautomeric Hydrogen Shift in Tropolone, J. J. Titman, Z. Luz and H. W. Spiess, J. Am. Chem. Soc., 114, 3756-3765 (1992).
  • Solid-state Reactions Studied By Carbon-13 Rotor-Synchronized Magic Angle Spinning Two-dimensional Exchange NMR 2. The Cope Rearrangement And Molecular Reorientation In Bullvalene, J. J. Titman, Z. Luz and H. W. Spiess, J. Am. Chem. Soc., 114, 3765-3771 (1992).
  • Increased Resolution In MAS NMR Spectra By Two-dimensional Separation Of Sidebands By Order, S. Féaux de Lacroix, J. J. Titman, A. Hagemeyer and H. W. Spiess, J. Magn. Reson., 97, 435-443 (1992).
  • Assessment of a Method for Measuring Heteronuclear Long-Range Coupling Constants, J. M. Richardson, J. J. Titman, J. Keeler and D. Neuhaus, J. Magn. Reson., 93, 533-553 (1991).
  • Structure and Conformation of a Phenoxylazolene Derivative Used in Studies of Antibodies Determined Using 1H NMR and Measurement of Long-Range (13C, 1H) Coupling Constants, J. J. Titman, J. Foote, J. Jarvis, J. Keeler and D. Neuhaus, Chem. Commun., 419-421 (1991).
  • Measurement of Homonuclear Coupling Constants from NMR Correlation Spectra, J. J. Titman and J. Keeler, J. Magn. Reson., 89, 640-646 (1990).
  • Selection of Coherence Transfer Pathways Using Inhomogeneous Adiabatic Pulses. Removal of Zero-Quantum Coherence, J. J. Titman, A. L. Davis, E. D. Laue and J. Keeler, J. Magn. Reson., 89, 176-183 (1990).
  • Measurement of Long-Range Heteronuclear Coupling Constants, J. J. Titman, D. Neuhaus and J. Keeler, J. Magn. Reson., 85, 111-131 (1989).
  • Suppression of Uninformative Peaks in Two-dimensional Relayed NOESY Spectra, J. Cavanagh, J. J. Titman and J. Keeler, Magn. Reson. Chem., 26, 1093-1096 (1988).
  • A Convenient Technique for the Measurement and Assignment of Long-Range Carbon-13 Proton Heteronuclear Coupling Constants, J. Keeler, D. Neuhaus and J. J. Titman, Chem. Phys. Lett., 146, 545-548 (1988).

Dr Jeremy Titman

School of Chemistry, University Park Nottingham, NG7 2RD


telephone: +44 (0) 115 951 3560

fax: +44 (0) 115 951 3562

email: jeremy.titman@nottingham.ac.uk